Separation, identification and quantification of the unsaponifiables of cottonseed oil and its deodorizer distillate

dc.contributor.authorMathur, Priyanka
dc.contributor.committeeChairKing, Clay
dc.contributor.committeeMemberRyu, Dojin
dc.contributor.committeeMemberMo, Huanbiao
dc.contributor.committeeMemberPrasad, Chandan
dc.date.accessioned2018-09-12T16:34:05Z
dc.date.available2018-09-12T16:34:05Z
dc.date.issued2011-12
dc.description.abstractThis study was conducted to separate, identify and quantify the unsaponifiables of cottonseed oil and its deodorizer distillate. The AOCS extraction method was used to separate the unsaponifiables from refined, bleached and deodorized (RBD) cottonseed oil and its deodorizer distillate. A silylation method was then used to identify and quantify the tocopherols and sterols which are the major components of the unsaponifiable materials of RBD cottonseed oil and its deodorizer distillate. Quantification of unsaponifiables was conducted using gas chromatography. The percentage of total unsaponifiables was found to be 2% in RBD cottonseed oil and 53.9% in the deodorizer distillate. The total tocopherols in RBD cottonseed oil were 3.6% of the total unsaponifiables (which included 2.3% α tocopherol and 1.37% β+γ tocopherol) and total sterols were 31.4% of total unsaponifiables (which included 1.8% stigmasterol, 2.3% campesterol and 27.2% β sitosterol). In the distillate, total tocopherols were 12.64% of the total unsaponifiables (which included 4.4% α tocopherol, 8.2 % β+γ tocopherols) and total sterols were 65.1% of total unsaponifiables (which included 1.2% stigmasterol, 6.6% campesterol and 57.3% β sitosterol).en_US
dc.identifier.urihttp://hdl.handle.net/11274/10350
dc.language.isoen_USen_US
dc.subjectPlant sciencesen_US
dc.subjectBiochemistryen_US
dc.subjectNutritionen_US
dc.titleSeparation, identification and quantification of the unsaponifiables of cottonseed oil and its deodorizer distillateen_US
dc.typeThesisen_US
thesis.degree.departmentNutrition and Food Scienceen_US
thesis.degree.disciplineFood Science
thesis.degree.grantorTexas Woman's Universityen_US
thesis.degree.levelMasteren_US
thesis.degree.nameMaster of Scienceen_US

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